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Ammonium Chloride
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Ammonium Chloride

Ammonium Chloride: CAS Number 12125-02-9, Molecular Formula: NH4Cl, Molecular Weight: 53.49

SPECIFICATIONS OF COMMERCIAL GRADE AMMONIUM CHLORIDE
CHARACTERISTIC Pure Pharma & Battery Grade Anti-caking & Uncoated
Dry Basis Assay (NH4Cl) Ammonium Chloride 99.5% minimum
Moisture 0.5% maximum
Iron 5 ppm maximum
Sulphate 0.015% maximum
Residue on Ignition 0.3% maximum
pH of 2% Solution 4.0-5.5
Matter insoluble in water 0.005% maximum
Heavy Metals as Pb 1 ppm maximum
Arsenic 1 ppm maximum
Packing will be 25/50kg in HMHDP bags placed in an HDPE bag or drum or in Jumbo bags or as desired by the buyer.

Ammonium Chloride FCC Food Grade
NH4Cl Formula weight 53.49

DESCRIPTION
Ammonium Chloride occurs as colorless crystals or as a white, fine or coarse, crystalline powder. It is somewhat hygroscopic. One gram dissolves in 2.6 mL of water at 25°, in 1.4 mL of boiling water, in about 100 mL of alcohol, and in about 8 mL of glycerin. The pH of a 1:20 solution is between 4.5 and 6.0.

REQUIREMENTS
Identification: A 1:10 aqueous solution gives positive tests for Ammonium and for Chloride.
Assay: Not less than 99.0% of NH4Cl after drying.
Lead: Not more than 4 mg/kg.
Loss on Drying: Not more than 0.5%.

Ammonium Chloride BP Ph Eur Grade Specifications
NH4Cl

DEFINITION
Content or Assay:99.0 per cent to 100.5 per cent (On dried substance basis).

CHARACTERS
Appearance:White or almost white, crystalline powder or colorless crystals.
Solubility: Freely soluble in water.

IDENTIFICATION
A. It gives the reactions of chlorides.
B. 10 ml of solution gives the reaction of ammonium salts.

TESTS
Solution S: A 10% solution: Appearance of solution: Solution is clear and colorless.
Acidity or alkalinity: To 10 ml of solution S add 0.05 ml of methyl red solution. Not more than 0.5 ml of 0.01 M hydrochloric acid or 0.01 M sodium hydroxide is required to change the color of the indicator.
Bromides and iodides: To 10 ml of solution S add 0.1 ml of dilute hydrochloric acid R and 0.05 ml of chloramine solution. After 1 min, add 2 ml of chloroform R and shake vigorously. The chloroform layer remains colorless.
Sulphates: Maximum 150 ppm.
Calcium: Maximum 200 ppm.
Iron: Maximum 20 ppm.
Heavy metals: Maximum 10 ppm.
Loss on drying: Maximum 1.0 per cent, determined on 1.00 g by drying in an oven at 105 °C for 2 h.
Sulphated ash: Maximum 0.1 per cent, determined on 2.0 g.


Ammonium Chloride USP
NH4Cl 53.49

Assay— Ammonium Chloride contains not less than 99.5 percent and not more than 100.5 percent of NH4Cl, calculated on the dried basis.
Packaging and storage— Preserve in tight containers.
Identification— A solution (1 in 10) responds to the tests for Ammonium and for Chloride
pH: between 4.6 and 6.0, in a solution (1 in 20).
Loss on drying— Dry it over silica gel for 4 hours: it loses not more than 0.5% of its weight.
Residue on ignition— Add 1 mL of sulfuric acid to about 2 g, accurately weighed, and heat the mixture gently until volatilization is complete: the residue is white, and when ignited, not more than 0.1% of nonvolatile substance remains.
Limit of thiocyanate— Acidify 10 mL of a solution (1 in 10) with hydrochloric acid, and add a few drops of ferric chloride TS: no orange-red color is produced.
Heavy metals: 0.001%.


Ammonium Chloride ACS Analytical Reagent
NH4Cl Formula Wt 53.49
CAS Number 12125–02–9

REQUIREMENTS
Assay: ≥99.5% NH4Cl
pH of a 5% solution: 4.5–5.5 at 25 °C

MAXIMUM ALLOWABLE
Insoluble matter: 0.005%
Residue after ignition: 0.01%
Calcium (Ca): 0.001%
Magnesium (Mg): 5 ppm
Heavy metals (as Pb): 5 ppm
Iron (Fe): 2 ppm
Phosphate (PO4): 2 ppm
Sulfate (SO4): 0.002%

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e-mail: info@foodoric.com

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Copyright Last 14 March, 2022

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