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Borax or Sodium Borate USP NF BP ACS Reagent Manufacturers Suppliers

Borax
Sodium Tetraborate Sodium Borate USP NF BP ACS Reagent
Borax

Sodium Borate or Borax CAS Number 1303-96-4, Molecular Formula: Na2B4O7-10H2O, Molecular Weight: 381.4

Sodium Borate USP NF Grade Specifications
Sodium Tetraborate, Borax
Na2B4O7-10H2O --- 381.37 --- [CAS 1303-96-4]
Anhydrous --- 201.22 [CAS 1330-43-4]

Sodium Borate contains an amount of Na2B4O7 equivalent to not less than 99.0 percent and not more than 105.0 percent of Na2B4O7·10H2O.

Identification: A solution (1 in 20) responds to the tests for Sodium and for Borate.
Carbonate and bicarbonate: To 5 mL of a solution (1 in 20), contained in a test tube, add 1 mL of 3 N hydrochloric acid: no effervescence is observed.
Heavy metals— the limit is 0.002%.


Borax BP Ph Eur Grade Specifications
Borax, Sodium Borate, Sodium Tetraborate
Na2B4O7-10H2O -- 381.4 -- CAS 1303-96-4

DEFINITION
Borax contains not less than 99.0 per cent and not more than the equivalent of 103.0  per cent of disodium tetraborate decahydrate.

CHARACTERS
A white, crystalline powder, colourless crystals or crystalline masses, efflorescent, soluble in water, very soluble in boiling water, freely soluble in glycerol.

IDENTIFICATION
A. To 1 ml of solution S (see Tests) add 0.1 ml of sulphuric acid and 5 ml of methanol \ and ignite. The flame has a green border.
B. To 5 ml of solution S add 0.1 ml of phenolphthalein solution. The solution is red. On the addition of 5 ml of glycerol (85 per cent) the colour disappears.
C. Solution S gives the reactions of sodium.

TESTS
Solution S: Dissolve 4.0 g in carbon dioxide-free water prepared from distilled water and  dilute to 100 ml with the same solvent.
Appearance of solution: Solution S is clear and colourless.
pH: The pH of solution S is 9.0 to 9.6.
Sulphates: 15 ml of solution S complies with the limit test for sulphates (50 ppm).
Ammonium: 6 ml of solution S diluted to 14 ml with water complies with the limit test for  ammonium (10 ppm).
Arsenic: 5 ml of solution S complies with limit test A for arsenic (5 ppm).
Calcium: 15 ml of solution S complies with the limit test for calcium (100 ppm).
Heavy metals: 12 ml of solution S complies with limit test A for heavy metals (25 ppm).


Sodium Borate Decahydrate or Borax ACS Reagent
Sodium Tetraborate Decahydrate ACS
Na2B4O7 -10H2O
Formula Wt 381.37
CAS Number 1303-96-4

REQUIREMENTS
Assay: 99.5-105.0% Na2B4O7-10H2O
pH of a 0.01 M solution: 9.15-9.20 at 25C

MAXIMUM ALLOWABLE
Insoluble matter: 0.005%
Chloride (Cl): 0.001%
Phosphate (PO4): 0.001%
Sulfate (SO4): 0.005%
Calcium (Ca): 0.005%
Heavy metals (as Pb): 0.001%
Iron (Fe): 5 ppm.

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Copyright Last 14 March, 2022

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